Validation of the analytical procedure for the determination of polyaromatic hydrocarbons in smoke flavourings using high performance liquid chromatography coupled to an ultraviolet, diode array or fluorescence detector

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作者：

C Brasseur，Franois Brose，A Pirlot，C Douny，G Eppe，G Maghuin-Rogister，ML Scippo

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摘要：

High performance liquid chromatography (HPLC) coupled to an ultraviolet (UV), diode array or fluorescence detector (UV/DAD/FLD) has been used to set up an analytical procedure for the quantification of 16 EU priority polyaromatic hydrocarbons (PAHs) in smoke flavourings. The following parameters have been determined for the 16 EU priority PAHs: limit of detection, limit of quantification, precision (repeatability and intermediate precision), recovery and measurement uncertainty, using the concept of accuracy profiles. They were in close agreement with quality criteria described in the Commission Regulation (EC) no. 627/2006 concerning PAHs in smoke flavourings.

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关键词：

Polyaromatic hydrocarbons PAH HPLC/UV/FLD Smoke flavouring Analytical procedure validation Accuracy profile Uncertainty measurement