Iron chloride enhancement of dimethylzinc-mediated radical conjugate addition of ethers and an amine to alkylidenemalonates
摘要：
The addition of FeCl 3 and the use of DMSO as a solvent enabled the radical conjugate addition of a cyclic acetal and a cyclic amine to alkylidenemalonates using a reagent amount (12.5 equiv) of the radical precursors to give Michael addition products in up to 84% yield. This represents a great improvement over the 5% yield obtained under the previously reported conditions.
展开
DOI：
10.1016/j.tetlet.2009.08.034
被引量：
年份：
2009
相似文献
参考文献
引证文献
来源期刊
Tetrahedron Letters
2009
引用走势
2010
被引量：13
辅助模式
0
引用
文献可以批量引用啦~
欢迎点我试用！
