AN IMPROVED SYNTHESIS OF 3-N-PENTADECYL CATECHOL (3-PDC)
摘要:
4-Alkoxymethyl-2-bromo-2-ethoxycarbonylbutanolides were obtained with good yields by the bromination of 4-alkoxymethyl-2-ethoxycarbonylbutanolides with bromine in dry carbon tetrachloride. Reaction of the products with thiourea and aryl-substituted thioureas gave spiroheteryl-fused lactones of a new generation-8-alkoxymethyl-3-amino(arylamino)-7-oxa-4-thia-2-azaspiro[4,4]-2-nonene-1,6-diones.
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DOI:
10.1080/00304947809355032
被引量:
年份:
1978
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1981
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