Electrochemical hydrogenation of citral
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20
摘要：
The factors (concentration of citral, composition of the solvent, AcOH <img src="/content/PJ74073628N43W2W/xxlarge8758.gif" alt="ratio" align="BASELINE" border="0"> citral ratio) affecting electrochemical hydrogenation of citral at an annealed copper cathode have been determined. The highest total yield (94 %) of the alcohols (nerol, geraniol, citronellol) with a considerable predominance of the latter is achieved at 40 % DMF in water, citral concentration 0.02M, and AcOH <img src="/content/PJ74073628N43W2W/xxlarge8758.gif" alt="ratio" align="BASELINE" border="0"> citral ratio=10<img src="/content/PJ74073628N43W2W/xxlarge8758.gif" alt="ratio" align="BASELINE" border="0">1. The transition to purely organic or purely aqueous media leads to a decrease in both the total yield of the alcohols and the selectivity of the process.
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DOI：
10.1007/BF00698998
被引量：
年份：
1993
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