Microwave assisted synthesis – a critical technology overview

阅读量:

176

作者:

M NuechterB OndruschkaW BonrathA Gum

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摘要:

Since 1986, when Gedye and Giguere published their first articles inTetrahedron Letterson microwave assisted syntheses in household microwave ovens, there has been a steadily growing interest in this research field. Since the use of microwaves comprises more than the simple application of a goal-oriented, innovative tool, it is crucial to be aware of the fundamentals of chemistry in the microwave field before investigating challenging reaction mechanisms. Therefore, the following overview focuses mostly on reaction engineering in the microwave field. Parallel reactions and scale-up are also discussed. The last section of this review is dedicated to the development of experimentally sound protocols on microwave-assisted syntheses and separations, which are illustrated through experiments.

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DOI:

10.1039/b310502d

被引量:

1107

年份:

2004

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来源期刊

Cheminform
20040304

引用走势

2006
被引量:130

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