Trinuclear Palladium(II) Complexes with 2‐Hydroxy‐4‐methoxyacetophenone N4‐Dimethylthiosemicarbazone: Synthesis, Spectral Studies and Crystal Structure of a Tripalladium Complex
摘要：
The synthesis and spectral characterization of a new triangular , trinuclear palladium(II) complex with the dianion of 2-hydroxy-4-methoxyacetophenone N 4 -dimethylthiosemicarbazone, 4MeOAp4Me is reported. The X-ray crystal structure determination of [Pd(4MeOAp4Me 2 )] 3 · DMSO shows it to contain a chair-type hexagon of alternating Pd and S atoms which form a molecular bowl. The crystal structure of H 2 4MeOAp4Me 2 shows that it is the E isomer with respect to the imine bond of the thiosemicarbazone moiety.
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DOI：
10.1002/(SICI)1099-0682(200004)2000:43.0.CO;2-R
被引量：
年份：
2000
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